XPS or ESCA Analysis:
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Depth profile MBE-deposited multi-layer structures on GaAs
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Determine stoichiometry of sputter-deposited or MOCVD materials
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Determine cause of soldering, bond pad, and adhesive bond difficulties
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Identify photoresist or wax residues, contaminants, and surface segregated impurities
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Measure thickness and determine uniformity of oxides, nitrides, or other film layers
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Depth profile multifilm contact structures on silicon or GaAs wafers
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Determine composition of thermal compounds or adhesives
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Evaluate the cleanliness of ceramic or plastic packaging materials
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Evaluate PCB laminate interfaces and surface conformal coatings
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Measure contamination on alumina feedthroughs and solve brazing problems
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Determine composition of electroplated gold and other metals, particularly on surfaces to which impurities migrate
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Chemistry of polyimide coating surface and effects on outgassing
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Identity cause of metallization layer delamination
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Detect and identify contaminants on connectors on plastic, ceramic, or pins
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Determine causes of corrosion
Infrared Spectroscopy or FTIR analysis:
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Identify flux residue
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Identify wax residue
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Identify thermal compound
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Identify adhesive
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Identify conformal coating
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Identify resin in circuit board
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Identify component plastics
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Identify polyimide coating
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Identify photo resist
TMA or Dilatometry:
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Measure thermal expansion properties of materials or IC packages
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Determine softening temperature of plastics & polymers or their degree of crystallinity
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Measure extent and temperature of plastic crystalline transitions
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Measure polymer or plastic glass transition temperature
DSC:
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Measure the specific heat of a material
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Measure energy of intermetallic phase formation
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Measure degree of cure of epoxy materials for electronic packaging or of epoxy adhesives
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Measure melting point temperature of solders, fluxes, waxes, sealants, and potting compounds
TGA or Thermogravimetry:
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Measure weight loss by outgassing
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Measure degree of water absorption
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Measure total fiberglass content in printed circuit boards
DMA:
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Measure glass transition temperature of printed circuit boards
Electrochemistry:
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Evaluate corrosion resistance of coated Kovar hermetic packages
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Strip coated metal layers to measure their thickness
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Measure corrosion rates and pitting potentials of contacts and pins
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Examine corrosion of electronics enclosures
Metallographic / Optical Microscopy / SEM:
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Cross-section analysis of solder joints, connectors, or ceramic capacitors
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Determine polysilicon grain sizes
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Check for voids in PCB material or in solder joints
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Determine whether copper foil layers have the proper surface characteristics in a PCB material
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Examine boards or wafers for anomalies
Profilometry:
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Step-height measurements of deposited layers / metallization films
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Surface roughness of metallic films
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